Author ORCID Identifier

N/A

N/A

https://orcid.org/0000-0001-7935-2532

N/A

Document Type

Article

Publication Date

2011

College/Unit

Eberly College of Arts and Sciences

Department/Program/Center

Chemistry

Abstract

Triazole–Au (TA–Au) catalysts were employed in several transformations involving propargyl ester rearrangement. Good chemoselectivity was observed, which allowed the effective activation of the alkyne without affecting the reactivity of the allene ester intermediates. These results led to the investigation of the preparation of allene ester intermediates with TA–Au catalysts under anhydrous conditions. As expected, the desired 3,3-rearrangement products were obtained in excellent yields (generally >90% yields with 1% loading). Besides the typical ester migrating groups, carbonates and carbamates were also found to be suitable for this transformation, which provided a highly efficient, practical method for the preparation of substituted allenes.

Source Citation

Wang, D., Zhang, Y., Cai, R., & Shi, X. (2011). Triazole–Au(I) complex as chemoselective catalyst in promoting propargyl ester rearrangements. Beilstein Journal of Organic Chemistry, 7, 1014–1020. https://doi.org/10.3762/bjoc.7.115

Comments

© 2011 Wang et al; licensee Beilstein-Institut.
This is an Open Access article under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
The license is subject to the Beilstein Journal of Organic Chemistry terms and conditions: (http://www.beilstein-journals.org/bjoc)

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